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Data are reported as follows: chemical shifts (ppm), multiplicity (s = singlet, d=doublet, t=triplet, q=quartet, sept.=septet, br=broad, m=multiplet, dd=doublet of doublets, ddd=doublet of doublet of doublets, dddd=doublet of doublet of doublet of doublets, dt=doublet of triplets, ddt=doublet of doublet of triplets, td=triplet of doublets), coupling constants (Hz), and integration